Unraveling Chemical Origins of Dendrite Formation in Zinc-Ion Batteries via In Situ/Operando X-Ray Spectroscopy and Imaging

In-situ scanning transmission X-ray microscopy (STXM) and spectro-ptychography are used to observe Zn dendrites and their chemical composition and distribution on the Zn surface during the stripping/plating progress are revealed.

Pourbaix Machine Learning Framework Identifies Acidic Water Oxidation Catalysts Exhibiting Suppressed Ruthenium Dissolution

A machine-learning-assisted computational pipeline is developed, and the Pourbaix energy for 2070 new oxides is screened to assess their electrochemical stability under acidic oxygen evolution reaction.

Superionic Conducting Vacancy-Rich Β-Li3n Electrolyte for Stable Cycling of All-Solid-State Lithium Metal Batteries

A superionic conducting, highly lithium-compatible, and air-stable vacancy-rich β-Li3N solid-state electrolyte is reported. It exhibited a high ionic conductivity, exceeding almost all the reported nitride-based solid-state electrolytes.

Nominally Identical Microplastic Models Differ Greatly in Their Particle-Cell Interactions

The nominally identical polystyrene microspheres from eight different manufacturers were significantly different in their ζ-potential, thus leading to different particle-cell interactions.

Single-Phase Local-High-Concentration Solid Polymer Electrolytes for Lithium-Metal Batteries

A class of locally high-concentration solid polymer electrolytes based on polymer blends is designed and the assembled cells can achieve a cycle life of 450 cycles.

A Novel Electrolyte for Long-Life Li Batteries

The cell assembled with this composite polymer electrolyte shows a prolonged cycle life of 1000 cycles at 1C.  


The spectromicroscopy (SM) facility at CLS has one beam line (10ID-1), enabling users to perform studies in the fields of polymer science, environmental science, and biological applications to novel material design and magnetic imaging. 

 

CLS-SM consists of an Apple II Elliptically Polarizing Undulator (EPU), a plane grating  monochromator (PGM), two branch lines, and two microscopes:

  •          Scanning Transmission X-ray Microscope (STXM)
  •          X-ray Photoemission Electron Microscope (X-PEEM)

 


List of Publications »

  • Prieto, E.R.; Sk, M.H.; Dwivedi, D.; Wang, J.; Barlow, B. et al. (2026). Comprehensive Near Edge X-ray Absorption Fine Structure analysis of corrosion in Iron at the nanoscale. Electrochimica Acta 574, 149358. 10.1016/j.electacta.2026.149358.
  • Zhang, Chunyang; Ngunjiri, Robert; Beinik, Igor; Schwenke, Jörg; Thånell, Karina et al. (2026). Chemical and Morphological Changes of Chloride-Affected Cu Catalysts during CO 2 Reduction Studied by In Situ Scanning Transmission Soft X-ray Microscopy. Journal of Physical Chemistry C 130(22) , 7615-7627. 10.1021/acs.jpcc.6c01560.
  • Das, Sambhu Charan; Chen, Kuan-Hung; Lin, Wei-Xuan; Wang, Hsiao-Tsu; Teng, Shu-Ang et al. (2026). Interfacial Robustness in Fe 2 TiO 5 /ZnO Core–Shell Nanodendrites Revealed by STXM-Ptychography for Enhanced Photoelectrochemical Performance. ACS Applied Materials and Interfaces 18(22) , 32011-32023. 10.1021/acsami.6c03568.